1 00:00:09,200 --> 00:00:11,800 Hi, I’m Jennifer Caban. 2 00:00:11,800 --> 00:00:13,566 Today I’m going to show you how to adjust 3 00:00:13,566 --> 00:00:17,333 user factors on your Vanta XRF analyzer. 4 00:00:17,333 --> 00:00:19,233 User factors allow you to adjust 5 00:00:19,233 --> 00:00:21,100 the factory default calibration 6 00:00:21,100 --> 00:00:23,800 to account for site specific matrix effects. 7 00:00:23,800 --> 00:00:26,766 You can do this using certified reference materials, 8 00:00:26,766 --> 00:00:28,766 your own internal standards, 9 00:00:28,766 --> 00:00:32,166 or samples that have been analyzed in a lab. 10 00:00:32,166 --> 00:00:34,600 In today’s example, silicone is reading 11 00:00:34,600 --> 00:00:37,300 a bit low on the Vanta on geological standards 12 00:00:37,300 --> 00:00:39,866 compared to the laboratory assays. 13 00:00:39,866 --> 00:00:41,900 It’s not uncommon to have to adjust 14 00:00:41,900 --> 00:00:44,066 the factory default calibration. 15 00:00:44,066 --> 00:00:45,666 When you do this you want 16 00:00:45,666 --> 00:00:48,266 to use at least three standards, 17 00:00:48,266 --> 00:00:49,866 but the more standards you use, 18 00:00:49,866 --> 00:00:52,333 the more robust the calibration. 19 00:00:52,333 --> 00:00:55,200 The first step is to test each of your standards 20 00:00:55,200 --> 00:00:59,933 with the Vanta XRF analyzer. 21 00:00:59,933 --> 00:01:03,100 Testing time can be either the same 22 00:01:03,100 --> 00:01:05,133 as your standard testing time 23 00:01:05,133 --> 00:01:07,166 or, to minimize statistical variation 24 00:01:07,166 --> 00:01:09,033 you can test for up to two to three times 25 00:01:09,033 --> 00:01:13,600 longer than standard testing times. 26 00:01:13,600 --> 00:01:18,100 This standard is assayed at about 26.0% silicone. 27 00:01:18,100 --> 00:01:28,266 We’ll see what result we’ll get with the Vanta. 28 00:01:28,266 --> 00:01:32,200 The test is complete and with the Vanta 29 00:01:32,200 --> 00:01:36,333 I’m reading about 22.8% silicone. 30 00:01:36,333 --> 00:01:38,733 I’m going to export that result 31 00:01:38,733 --> 00:01:41,200 along with the results on my other standards 32 00:01:41,200 --> 00:01:43,466 and compare that in an X/Y plot 33 00:01:43,466 --> 00:01:46,133 to the laboratory assays. 34 00:01:46,133 --> 00:01:48,900 I’ve done that here in an Excel® spreadsheet. 35 00:01:48,900 --> 00:01:52,166 I have the Vanta XRF results on the X axis 36 00:01:52,166 --> 00:01:55,800 and the laboratory assays on the Y axis. 37 00:01:55,800 --> 00:01:58,900 I’ve also enabled the display equation feature 38 00:01:58,900 --> 00:02:01,866 on the graph so that I have a slope 39 00:02:01,866 --> 00:02:04,500 and a Y intercept of my line. 40 00:02:04,500 --> 00:02:07,066 These are the values that I’m then going to import 41 00:02:07,066 --> 00:02:13,000 into the user factors menu on the Vanta. 42 00:02:13,000 --> 00:02:15,166 Going back to the Vanta, 43 00:02:15,166 --> 00:02:17,600 I’m going to swipe down on the right hand side 44 00:02:17,600 --> 00:02:22,200 and select the User Factors option. 45 00:02:22,200 --> 00:02:25,333 I’m going to create a model 46 00:02:25,333 --> 00:02:31,100 which I’ll call Si for silicone. 47 00:02:31,100 --> 00:02:33,166 I’m then going to take the slope 48 00:02:33,166 --> 00:02:36,466 and the Y intercept from the line I plotted in Excel® 49 00:02:36,466 --> 00:02:41,400 and input those in as the factor and the offset. 50 00:02:41,400 --> 00:02:49,333 The factor was one point one one nine nine. 51 00:02:49,333 --> 00:02:51,800 For the offset, I plotted this in Excel® 52 00:02:51,800 --> 00:02:54,366 as a percent but the Vanta is calling for it 53 00:02:54,366 --> 00:02:55,800 as parts per million. 54 00:02:55,800 --> 00:02:57,633 So I need to convert that percent value 55 00:02:57,633 --> 00:03:00,366 to parts per million in order to input it. 56 00:03:00,366 --> 00:03:09,333 The converted value is seventeen thousand twenty seven. 57 00:03:09,333 --> 00:03:11,000 And that’s it, I’ve now created 58 00:03:11,000 --> 00:03:13,366 the user factor model on my Vanta. 59 00:03:13,366 --> 00:03:15,033 I can now go back and test 60 00:03:15,033 --> 00:03:24,766 my standard with the new model. 61 00:03:24,766 --> 00:03:27,866 Recall that the assayed value for this standard 62 00:03:27,866 --> 00:03:30,300 is about 26.0% silicone and when 63 00:03:30,300 --> 00:03:35,600 I first tested the sample I was getting about 22.8% silicone. 64 00:03:35,600 --> 00:03:37,133 We’ll see what we get with the 65 00:03:37,133 --> 00:03:45,233 new user factor model enabled. 66 00:03:45,233 --> 00:03:49,500 With the new model I’m getting about 26.9% silicone 67 00:03:49,500 --> 00:03:51,200 which is significantly closer to the 68 00:03:51,200 --> 00:03:53,866 assayed value of 26.0%. 69 00:03:53,866 --> 00:03:55,000 And that’s it, 70 00:03:55,000 --> 00:03:56,600 that’s how you create user factors 71 00:03:56,600 --> 00:03:58,633 on the Vanta XRF analyzer. 72 00:03:58,633 --> 00:04:00,533 Thanks for watching!