1 00:00:08,633 --> 00:00:11,366 Hi, I’m Andrew Cardamone. 2 00:00:11,366 --> 00:00:13,200 Today I’m going to talk to you about what it means 3 00:00:13,200 --> 00:00:15,300 when you get no match during your alloy testing 4 00:00:15,300 --> 00:00:17,700 using the Vanta XRF analyzer. 5 00:00:17,700 --> 00:00:19,333 I will also discuss how to obtain 6 00:00:19,333 --> 00:00:21,933 the appropriate grade match for your sample. 7 00:00:21,933 --> 00:00:38,633 In today’s example I’ll be analyzing a nickel alloy, MonelK500. 8 00:00:38,633 --> 00:00:41,133 As you can see, no grade to compare 9 00:00:41,133 --> 00:00:43,166 has appeared across the top of the screen. 10 00:00:43,166 --> 00:00:44,500 Let’s take a look at the chemistry 11 00:00:44,500 --> 00:00:46,633 to better understand what might be going on here. 12 00:00:46,633 --> 00:00:48,633 We are clearly analyzing a nickel alloy, 13 00:00:48,633 --> 00:00:50,366 so why didn’t we get a match? 14 00:00:50,366 --> 00:00:54,833 The most common reason for no match to occur is sample contamination. 15 00:00:54,833 --> 00:00:58,333 This can happen when a sample is painted, plated or coated. 16 00:00:58,333 --> 00:01:01,133 Since we’re working with a known alloy standard however, 17 00:01:01,133 --> 00:01:03,833 contamination doesn’t seem to be our issue. 18 00:01:03,833 --> 00:01:06,300 Although it’s far less common, 19 00:01:06,300 --> 00:01:08,600 the sample not being included in the grade library 20 00:01:08,600 --> 00:01:10,933 can also cause no match to occur. 21 00:01:10,933 --> 00:01:15,166 To check if this is the case open the grade match icon. 22 00:01:15,166 --> 00:01:17,300 Scroll down to the libraries. 23 00:01:17,300 --> 00:01:22,466 Select the library, and open the list. 24 00:01:22,466 --> 00:01:24,833 We can see here that MonelK500 is indeed 25 00:01:24,833 --> 00:01:26,966 included in our active library. 26 00:01:26,966 --> 00:01:28,766 So we’ve ruled out contamination 27 00:01:28,766 --> 00:01:31,033 and our sample is in the active library. 28 00:01:31,033 --> 00:01:33,100 So what else can we do to get a match? 29 00:01:33,100 --> 00:01:38,000 Lets go back to the grade match page. 30 00:01:38,000 --> 00:01:39,933 You’ll notice across the top that it says 31 00:01:39,933 --> 00:01:42,033 show match number less than 4. 32 00:01:42,033 --> 00:01:44,033 The match number is an indication of how closely 33 00:01:44,033 --> 00:01:45,766 the chemistry of your sample matches 34 00:01:45,766 --> 00:01:48,266 the chemistry specified in the grade library. 35 00:01:48,266 --> 00:01:50,633 A value of 1 indicates a very good match 36 00:01:50,633 --> 00:01:53,066 whereas a value of 10 indicates a poor match. 37 00:01:53,066 --> 00:01:56,200 Let’s increase our value to 6 38 00:01:56,200 --> 00:02:11,800 and re-test our sample. 39 00:02:11,800 --> 00:02:13,600 You can see now that we’ve successfully 40 00:02:13,600 --> 00:02:16,566 identified the material as MonelK500. 41 00:02:16,566 --> 00:02:18,466 You’ll also notice that below the sample name 42 00:02:18,466 --> 00:02:20,300 there’s a small value of 5.0. 43 00:02:20,300 --> 00:02:22,233 That is the match number. 44 00:02:22,233 --> 00:02:24,033 Since we previously specified the match number 45 00:02:24,033 --> 00:02:26,900 had to be less than 4, we obtained no match. 46 00:02:26,900 --> 00:02:29,100 Now that we’ve increased our match number to 6, 47 00:02:29,100 --> 00:02:31,066 we are able to obtain a match. 48 00:02:31,066 --> 00:02:33,066 In our case, since we are comparing 49 00:02:33,066 --> 00:02:35,633 our sample to a single alloy grade, 50 00:02:35,633 --> 00:02:38,533 we are able to refine the search even further. 51 00:02:38,533 --> 00:02:42,666 To do that, once again open the grade match icon. 52 00:02:42,666 --> 00:02:45,733 Scroll down to the grade compare and select. 53 00:02:45,733 --> 00:02:48,600 Right now the Vanta is set up with Best Match. 54 00:02:48,600 --> 00:02:51,133 What this does is it compares our sample 55 00:02:51,133 --> 00:02:52,866 with all the grades in the grade library, 56 00:02:52,866 --> 00:02:55,566 and finds the best match within that grade library. 57 00:02:55,566 --> 00:02:58,533 To further refine this we can hit selected grade 58 00:02:58,533 --> 00:03:02,266 and then choose our sample, MonelK500. 59 00:03:02,266 --> 00:03:05,100 By doing so the Vanta will now compare our sample 60 00:03:05,100 --> 00:03:10,066 to just the specifications for MonelK500. 61 00:03:10,066 --> 00:03:23,766 Lets re-test our sample. 62 00:03:23,766 --> 00:03:25,666 Looking at the chemistry we can see that 63 00:03:25,666 --> 00:03:28,100 nickel and copper are outlined in red. 64 00:03:28,100 --> 00:03:29,833 This outline indicates that they are outside 65 00:03:29,833 --> 00:03:32,833 the specification range for MonelK500. 66 00:03:32,833 --> 00:03:35,066 This is why we initially obtained no match, 67 00:03:35,066 --> 00:03:36,933 our sample is out of spec. 68 00:03:36,933 --> 00:03:38,633 The red outline allows you to quickly see 69 00:03:38,633 --> 00:03:41,133 which elements are causing your sample to fall out of spec, 70 00:03:41,133 --> 00:03:42,800 and to make any process changes 71 00:03:42,800 --> 00:03:44,833 that need to be made to correct this. 72 00:03:44,833 --> 00:03:46,666 You may also notice during testing 73 00:03:46,666 --> 00:03:48,666 that initially a match is shown, 74 00:03:48,666 --> 00:03:51,766 but then as the test finishes, no match appears. 75 00:03:51,766 --> 00:03:55,266 This occurs because as the precision decreases over time, 76 00:03:55,266 --> 00:03:58,133 and the amount outside of the specification increases, 77 00:03:58,133 --> 00:03:59,900 we penalize the match number more, 78 00:03:59,900 --> 00:04:02,766 and that results in no match being displayed. 79 00:04:02,766 --> 00:04:04,633 I hope explaining what no match means 80 00:04:04,633 --> 00:04:06,466 has been useful for your alloy testing. 81 00:04:06,466 --> 00:04:07,966 Thank you for watching.